Sergey S. Zalesskiy†, Ernesto Danieli‡, Bernhard Blümich*‡, and Valentine P. Ananikov*†§† Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, 119991, Russia‡ Institut für Technische Chemie und Makromolekulare Chemie, RWTH Aachen University, Worringerweg 1, D-52074 Aachen, Germany§ Department of Chemistry, Saint Petersburg State University, Stary Petergof, 198504, RussiaChem. Rev., Article ASAPDOI: 10.1021/cr400063gPublication Date (Web): April 29, 2014
Reaction monitoring using inductive ESI mass spectrometry allows chemical reactions to be tracked in real time, including air- and moisture-sensitive as well as heterogeneous reactions. Highly concentrated solutions can also be monitored for long periods without emitter clogging. Sheath gas assists in nebulization and a sample splitter reduces the delay time and minimizes contamination of the instrument. Short-lived intermediates (ca. 5 s) were observed in Pd/C-catalyzed hydrogenolysis, and several intermediates were seen in Negishi cross-coupling reactions.
Xin Yan, Ewa Sokol, Dr. Xin Li, Guangtao Li, Dr. Shiqing Xu andProf. R. Graham Cooks* Angewandte Chemie International Edition
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